Novel bis ligand namely 2,2'-(4,4'-(4,4'-methylenebis(4,1-phenylene)bis (diazene-2,1-diyl))bis(4,1- phenylene))bis(azanediyl)bis(oxomethylene)dibenzoic acid (ADM) has been prepared and characterized. The coordination polymers based on this bis ligand with transition metal ions like Cu+2,Co+2,Ni+2,Mn+2and Zn+2 were prepared and characterized on the basis of elemental analyses, infrared spectra, electronic spectra, magnetic measurements and thermogravimetric analyses. All the coordination polymers are insoluble in acetone, ethanol, chloroform, methanol, benzene, DMF and DMSO. All the novel synthesized compounds were screened for their antibacterial and antifungal activities.
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