The research methods on the vacillator’s development quantitative determination of in substance and suppositories by absorption spectrophotometer were conducted and there was chosen an optimal solvent and dilution stability and also was investigated an optical density over time, and concentration range (2·10-6_ 2·10-5 g / ml) was set, where the linear dependence of the optical density concentration was performed. The developed technique allows controlling composition and technology of suppositories with acyclovir and oils in an industrial environment
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