Phytochemical investigation of the roots of Wattakaka volubilis led to the isolation of steroid like β-sitosterol; a triterpenoid aglyconedrevogenin A; fatty acid 9, 12 – octadecadienoic acid; a phenolic compound quinic acid; aromatic ester 1, 2 – benzenedicarboxylic acid diisooctyl ester; a flavonoid 5, 7 – dihydroxy – 6, 8 – dimethoxyflavone; an alkaloid N-[4-bromo-n-butyl]-2-piperidinone and a desoxy sugar digitoxose from the ethanolic extract. IR, 1HNMR and EI-MS spectrometric data were used for the characterization of above mentioned compounds. All these eight compounds have been reported for the first time from the roots of Wattakaka volubilis
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